Kyushu University / Hata Laboratory

STEM-ACOM / Nanobeam diffraction mapping

Nanoscale Microstructural Analysis by STEM Automated Crystal Orientation Mapping

STEM-ACOM (Automated Crystal Orientation Mapping) is a method that scans a finely focused electron beam in a TEM and analyzes crystal orientation and phase from electron diffraction patterns acquired at each point. It is effective for local orientation analysis of microstructures, thin films, nanocrystals, and heavily deformed materials where EBSD lacks sufficient spatial resolution. Our laboratory analyzes nanoscale texture, grain boundaries, and orientation distributions in superconducting thin films, drawn pearlitic steels, magnetic thin films, and related materials.

Key Points

Nanoscale orientation mapping

We visualize the orientation distribution of fine grains and columnar structures using nanometer-scale electron diffraction data.

Linking texture to functional properties

We quantitatively evaluate crystal orientations that govern functional properties, such as c-axis texture and low-angle grain-boundary networks in superconducting thin films.

Applications to heavily deformed materials and thin films

We apply this approach to nanostructures that are difficult to analyze by conventional methods, including drawn pearlitic steel and FePt-C thin films.

Related Publications and Information

Selected publications and related information on this topic are listed below.